Browse Data ESRA-CYC-0001 Cycling Public ⚠ Incomplete — 3 fields missing
Katherine Steinberg
0000-0002-8232-7714
Betar Gallant
Deciphering Unresolved Materials in Quantitative Analysis of Lithium Metal Solid Electrolyte Interphases
2025_KatherineSteinberg_BetarGallant_ACS.Energy.Lett._5c01274 ← click to see all uploads from this cell
10.1021/acsenergylett.5c01274 ↗
2026-08-12 21:51:56
c4848812-829f-49bc-8c24-57070547af74
How to Cite
1 — Cite the dataset paper
↗ View paper
2 — Cite the ESRA platform
Galib, M. et al. (2026). ESRA: Energy Storage Research Assistant. Argonne National Laboratory. https://github.com/MusannaGalib/esra-platform
CC BY 4.0  ·  Data shared under Creative Commons Attribution 4.0

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Linked Uploads

Type Group Date Project Link
SEM Betar Gallant 2026-08-14 12:55 Deciphering Unresolved Materials in Quantitative Analysis of Lithium Metal Solid Electrolyte Interphases same cell
NMR Betar Gallant 2026-08-12 21:52 Deciphering Unresolved Materials in Quantitative Analysis of Lithium Metal Solid Electrolyte Interphases same cell
ICP Betar Gallant 2026-08-12 21:52 Deciphering Unresolved Materials in Quantitative Analysis of Lithium Metal Solid Electrolyte Interphases same cell
GC Betar Gallant 2026-08-12 21:51 Deciphering Unresolved Materials in Quantitative Analysis of Lithium Metal Solid Electrolyte Interphases same cell

Materials Studied 6 materials

Material Family Role(s) Ion
1 M LiPF6 in EC/DEC (LP40)  · LP40 carbonate electrolyte Carbonate
Liquid
 Electrolyte Li
1 M LiFSI in DME  · Ether electrolyte Ether / glyme
Liquid
 Electrolyte Li
0.6 M LiDFOB + 0.2 M LiBF4 in FEC/DEC (1:2)  · Fluorinated borate electrolyte Carbonate
Liquid
 Electrolyte Li
LiFSI in DME/TTE  · Localized high-concentration electrolyte Localized high-concentration
Liquid
 Electrolyte Li
Li metal  · Lithium metal
SEI quantified by GC, ICP and NMR titration
 Alkali metal
Anode
 Anode Li
Cu foil  · Copper working electrode Current-collector metal
Other
 Working electrode, Current collector —

Declared for sample 2025_KatherineSteinberg_BetarGallant_ACS.Energy.Lett._5c01274 — shared by every dataset on this sample.

Experiment Metadata

Visibility public
Electrolyte Multiple: LP40; LiFSI DME; LiDFOB + LiBF₄ FEC/DEC; LiFSI DME/TTE LHCE
Temperature C 25.0
Anode Material Li chips (99.9%, 16 mm × 0.6 mm, MTI Corp; rolled to ~4× original size)
Publication Doi 10.1021/acsenergylett.5c01274
Number Of Cycles Variable per electrolyte to achieve 0.6–0.8 mAh total capacity loss (LP40: 4; LiFSI DME: 6; LiDFOB+LiBF₄: 9; LiFSI LHCE: 12 for ¹H-NMR)
Cathode Material Cu foil (16 mm diameter, working electrode)
Institution Code ESRA
Electrode Area Cm2 0.0
Voltage Window — Lower 0.0
Voltage Window — Upper 1.0
Theoretical Capacity Mah 3860.0
Current / C-Rate / Protocol Summary Constant-capacity galvanostatic protocol; 5 h initial rest; j = 0.5 mA/cm², Q = 1 mAh/cm²; stripped to 1 V vs. Li; 5 min rest between each half cycle