Browse Data ESRA-NMR-0001 NMR Public
Katherine Steinberg
0000-0002-8232-7714
Betar Gallant
Deciphering Unresolved Materials in Quantitative Analysis of Lithium Metal Solid Electrolyte Interphases
2025_KatherineSteinberg_BetarGallant_ACS.Energy.Lett._5c01274 ← click to see all uploads from this cell
10.1021/acsenergylett.5c01274 ↗
2026-08-12 21:52:03
e4f9d892-b173-47dd-8008-c932886e087b
How to Cite
1 — Cite the dataset paper
↗ View paper
2 — Cite the ESRA platform
Galib, M. et al. (2026). ESRA: Energy Storage Research Assistant. Argonne National Laboratory. https://github.com/MusannaGalib/esra-platform
CC BY 4.0  ·  Data shared under Creative Commons Attribution 4.0

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Linked Uploads

Type Group Date Project Link
SEM Betar Gallant 2026-08-14 12:55 Deciphering Unresolved Materials in Quantitative Analysis of Lithium Metal Solid Electrolyte Interphases same cell
ICP Betar Gallant 2026-08-12 21:52 Deciphering Unresolved Materials in Quantitative Analysis of Lithium Metal Solid Electrolyte Interphases same cell
GC Betar Gallant 2026-08-12 21:51 Deciphering Unresolved Materials in Quantitative Analysis of Lithium Metal Solid Electrolyte Interphases same cell
Cycling Betar Gallant 2026-08-12 21:51 Deciphering Unresolved Materials in Quantitative Analysis of Lithium Metal Solid Electrolyte Interphases same cell

Materials Studied 6 materials

Material Family Role(s) Ion
1 M LiPF6 in EC/DEC (LP40)  · LP40 carbonate electrolyte Carbonate
Liquid
 Electrolyte Li
1 M LiFSI in DME  · Ether electrolyte Ether / glyme
Liquid
 Electrolyte Li
0.6 M LiDFOB + 0.2 M LiBF4 in FEC/DEC (1:2)  · Fluorinated borate electrolyte Carbonate
Liquid
 Electrolyte Li
LiFSI in DME/TTE  · Localized high-concentration electrolyte Localized high-concentration
Liquid
 Electrolyte Li
Li metal  · Lithium metal
SEI quantified by GC, ICP and NMR titration
 Alkali metal
Anode
 Anode Li
Cu foil  · Copper working electrode Current-collector metal
Other
 Working electrode, Current collector —

Declared for sample 2025_KatherineSteinberg_BetarGallant_ACS.Energy.Lett._5c01274 — shared by every dataset on this sample.

Experiment Metadata

Nucleus ¹H (separator extract in DMSO-d6); ¹⁹F (wash solvent anions; LiF); ⁷Li (wash solvent cations)
Solvent DMSO-d6 for separator NMR; DMC or DME for wash solvent; water for LiF
Visibility public
Temperature C 6.0
Nmr Experiment ¹⁹F: 64k FID, 32 scans, 8 s relaxation delay, 20 ppm SW (−77 ppm LiPF₆; 52 ppm LiFSI; −150 ppm LiDFOB/LiBF₄); ⁷Li: 16k FID, 8 scans, 5 s relaxation delay, 30 ppm SW (0 ppm); LiF ¹⁹F: 64k FID, 32 scans, 8 s realization delay, 20 ppm SW (−120 ppm)
Publication Doi 10.1021/acsenergylett.5c01274
Institution Code ESRA
Field Strength Mhz 500.34
Reference Standard none