Name: ESRA-ICP-0004: Inductively Coupled Plasma spectroscopy of Cell trial-data
Creator: Musanna Galib
Published: 2026-10-20
License: https://spdx.org/licenses/CC-BY-4.0

Researcher

Musanna Galib

ORCID

0000-0002-1735-7546

PI(s)

Betar M. Gallant

Project

Energy Storage Research Alliance

Sample ID

trial-data ← click to see all uploads with this sample ID

Publication DOI

Not published yet

Notes

Batch run analyzing many samples (150_01, 150_03-150_13, 153_03-153_06) in one session. None are the same physical cell as this upload's Cycling data (cell 204). Electrolyte is confirmed as LP40 only for 153_05 and 153_06 (cyc_num_metadata.csv); the 150_xx rows have no matching spreadsheet entry, so their electrolyte is not stated anywhere in the attached files. cell_id is left out because this block covers many distinct cells, not one.

Upload Date (CDT)

2026-10-20 23:56:01

Upload ID

9c2f1fae-53cd-4095-9ea9-00d643a383f6

How to Cite

1 — Cite the dataset paper

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2 — Cite the ESRA platform

Galib, M. et al. (2026). ESRA: Energy Storage Research Assistant. Argonne National Laboratory. https://github.com/MusannaGalib/esra-platform

CC BY 4.0 · Data shared under Creative Commons Attribution 4.0

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PI Name(s)

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Sample ID

Publication DOI

Notes

ICP fields

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Instrument Type *

Elements Measured *

Calibration Range

Digestion Method

Matrix

Materials studied

Shared by all 8 datasets on trial-data. Edits apply to every one.

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Storage LocationNERSC Community File System

Path

/global/cfs/cdirs/m4845/gsharing/_training/betar-m-gallant/energy-storage-research-alliance/trial-data/04_ICP_DATA/icp/ESRA-ICP-0004/

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Linked Uploads

Other datasets with the same sample ID (trial-data).

Type	Group	Date	Project	Link
SEM	Betar M. Gallant	2026-10-20 23:56	Energy Storage Research Alliance	same sample
ICP	Betar M. Gallant	2026-10-20 23:56	Energy Storage Research Alliance	same sample
GC	Betar M. Gallant	2026-10-20 23:55	Energy Storage Research Alliance	same sample
SEM	Betar M. Gallant	2026-10-20 23:21	Energy Storage Research Alliance	same sample
GC	Betar M. Gallant	2026-10-20 23:20	Energy Storage Research Alliance	same sample

Materials Studied 6 materials

Material	Family	Role(s)	Ion
Li Purchased / commercial Cell assembly Other notes: Rolled out to approximately 4x original chip size	Alkali metal Anode	Anode, Counter electrode	Li
Cu Purchased / commercial Electrode fabrication Wash solvent: acetone Wash solvent: Milli-Q water Wash solvent: 1 M HCl (aq), Fisher ACS Plus Vacuum dry duration: overnighttemperature: 50 °C	Current-collector metal Other	Working electrode, Current collector	—
Celgard 2325 Purchased / commercial Cell assembly Vacuum dry duration: overnighttemperature: 50 °C	Separator material Other	Separator	—
LP40 Confirmed for ICP rows 153_05/153_06 and 156_03/156_04 via cyc_num_metadata.csv; not confirmed for every row in the two ICP files included in this upload. Source: SI, Experimental Methods > Materials, p.17. Purchased / commercial Sigma Aldrich · battery grade, used as received	Carbonate Liquid	Electrolyte	Li
LiFSI DME Salt concentration / exact ratio not stated in the available SI pages — only the name "LiFSI DME" is used throughout. LiFSI itself: 99.9+%, Arkema, vacuum dried at 120 °C (SI, Materials, p.17). Used for cell 261_01 (cyc_num_metadata.csv: electrolyte=fsidme, cyc=6, matching the SI's '6 cycles for LiFSI DME' target). Made in this work Electrolyte preparation	Ether / glyme Liquid	Electrolyte	Li
LiFSI DME/TTE LHCE Salt concentration / DME:TTE ratio not stated in the available SI pages — only the qualitative name is used (e.g. Figure S3a caption). Used for cell 204_01 (cyc_num_metadata.csv: electrolyte=lhce, cyc=12, matching the SI's '12 cycles for LiFSI DME/TTE LHCE' target). Made in this work Electrolyte preparation	Localized high-concentration Liquid	Electrolyte	Li

Declared for sample trial-data — shared by every dataset on this sample.

Experiment Metadata

Matrix	3 wt% HCl
Visibility	public
Matrix Source	SI, ICP-AES, p.18
Instrument Type	ICP-AES; Agilent 5100 VDV
Digestion Method	Not an acid digestion of a solid: liquid wash-solvent sample diluted 1:1 with Milli-Q water, filtered through a 0.22 micron hydrophilic PTFE syringe filter, then 0.4 mL added to 4 mL of 3 wt% HCl
Institution Code	ESRA
Calibration Range	0, 5, 10, 25, 30, 50, 75, 100 mM LiCl, each in 4 mL 3 wt% HCl; recalibrated each time the plasma was reignited
Elements Measured	Li, P
Instrument Type Source	SI, Experimental Methods > ICP-AES, p.18
Digestion Method Source	SI, ICP-AES, p.18
Calibration Range Source	SI, ICP-AES, p.18
Elements Measured Source	240614_150_153.txt column headers (Li610.362nm, Li670.784nm, P213.618nm, P214.914nm, P253.565nm)

Uploaded Files 2 files · 1.7 kB

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v1 (latest)

2026-10-21 04:56 UTC

published at upload · ESRA (automatic)

2 files · 1.7 kB

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